Shimadzu Uv 2401Pc | How To Operate The Uv 2401 Pc Recording Spectrophotometer 78 개의 베스트 답변

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Shimadzu Corporation – UV-2401PC/UV-2501PC

The UV-2401PCA Superbly Engineered InstrumentThis single monochromator system proves the analyst with the reliability and performance our customers have …

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Shimadzu UV 2401PC Spectrophotometer

The Shimadzu UV 2401PC Spectrophotometer is a single monochromator system proving the analyst with the reliability and performance our customers have come …

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Shimadzu UV-2401 Dual-Beam UV-Vis Spectrophotometer …

The Shimadzu UV-2401 PC UV-Visible Spectrometer is a double-beam instrument allowing accurate measurement of absorbance spectra and quantitative measurement …

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Shimadzu UV-2401PC – International Equipment Trading Ltd

Shimadzu UV-2401PC UV-VIS recording spectrophotometer (p/n 206-82301-92)

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I Read the instruction manual thoroughly before you use the …

UV-Visible Spectrophotometer. Model name. : UV-2401 PC. UV-2501 PC. Manufacturer. : SHIMADZU CORPORATION. ANALYTICAL INSTRUMENTS DIVISION. Address.

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Lidstrom:UV-2401PC UV-Vis recording spectrophotometer

About the UV-2401 PC spectrophotometer. Manual; Shimadzu = manufacturer. TUTORIALS: kinetics tutorial · software turorial for “UV Probe” software …

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How to Operate the UV 2401 PC Recording Spectrophotometer
How to Operate the UV 2401 PC Recording Spectrophotometer

주제에 대한 기사 평가 shimadzu uv 2401pc

  • Author: William Hoover
  • Views: 조회수 468회
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  • Date Published: 2018. 3. 22.
  • Video Url link: https://www.youtube.com/watch?v=829o9rMYVTQ

UV-2401PC/UV-2501PC ( Shimadzu Corporation )

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The establishment of EVISA is funded by the EU through the Fifth Framework Programme (G7RT- CT- 2002- 05112).

Supporters of EVISA includes:

Shimadzu UV 2401PC Spectrophotometer

The Shimadzu UV 2401PC Spectrophotometer is a single monochromator system providing the analyst with the reliability and performance our customers have come to expect in Shimadzu instruments. The systems low stray light/wide dynamic range/small beam size combination makes this instrument well suited to handle a variety of practical situations. From small sample volumes to highly absorbing samples, the software gives you the power and versatility of an extremely sophisticated system in a package that’s easy to learn and use.

Specifications:

– Wavelength range: 190 to 900nm (performance guaranteed range). Extendable to 1,100nm through the use of the optional photomultiplier. (The measurable range may be restricted in the shorter wavelength side depending on the type of photomultiplier used.)

– Monochromator system: UV-2401PC: Single monochromator with a high-performance blazed holographic grating in the aberration corrected Czerny-Turner mounting.

UV-2501PC: Double monochromator with a high-performance double-blazed holographic grating in the aberration corrected Czerny-Turner mounting.

– Resolution: 0.1nm.

– Spectral bandwidth: 0.1, 0.2, 0.5, 1, 2 and 5nm.

– Wavelength repeatability: ±0.1nm.

– Wavelength accuracy: ±0.3nm.

– Wavelength scanning speed: FAST, MEDIUM, SLOW and SUPER SLOW.

– Light source: 50W halogen lamp (2,000 hours life) and D2 lamp (500 hours life).

– Light source lamp switching: Selectable between 282nm and 393nm.

– Stray light: Less than 0.015% at 220nm and 340nm.

– Detector: Photomultiplier R-928.

– Photometric system: Double-beam, direct ratio system with dynode feedback.

– Photometric mode: Absorbance (Abs.), transmittance (%), reflectance (%) and energy (E).

– Photometric range: Absorbance : -4~5 Abs. (0.001 Abs. increments).

– Transmittance: 0~999.9% (0.01% increments).

– Reflectance: 0~999.9% (0.01% increments).

– Photometric accuracy: ±0.002 Abs. (0~0.5 Abs.) with NIST 930D Filter, ±0.004 Abs. (0.5~1 Abs.) with NIST 930D Filter, ±0.3%T (0~100%T) with NIST 930D Filter.

– Photometric repeatability: ±0.001 Abs. (0~1.0 Abs.), ±0.1%T.

– Baseline correction: Selectable with storage in firmware.

– Baseline flatness: Within ±0.001 Abs. (excluding noise; 2nm slit width and SLOW wavelength scanning speed).

– Drift: Less than 0.0004 Abs. per hour (after 2 hours warm-up).

– Power requirements: 100V, 120V, 220V, 240V, switch-selectable; 50/60Hz; 250 VA.

– Dimensions and weight: Main spectrophotometer 570W X 660D X 275Hmm; about 36kg.

– Software Specifications: Personal Spectroscopy Software (standard), Spectrum, Quantitative, Time Course.

Shimadzu UV-2401 Dual-Beam UV-Vis Spectrophotometer and Computer – My Lab Store

The Shimadzu UV-2401 PC UV-Visible Spectrometer is a double-beam instrument allowing accurate measurement of absorbance spectra and quantitative measurement. Software enhancements allow for complex calculations, comparisons, and conversions etc. This item is tested (as shown in images) and comes with a 90-day warranty.

Shimadzu UV-2401PC UV-VIS recording spectrophotometer (p/n 206-82301-92)

Refurbished Shimadzu UV-2401PC UV-VIS recording spectrophotometer (p/n 206-82301-92). OPTIONAL: Shimadzu UV Probe PC workstation & Shimadzu CPS-240A cell positioner (p/n 204-05837-92). Please contact us for complete Shimadzu UV 2401 details. (UV2401)

System Specifications

*Optical System: Double-beam

*Spectral Bandwidth: 0.1, 0.2, 0.5, 1, 2 and 5nm

*Wavelength Range: 190 to 900nm

*Accuracy: ±0.3nm

*Repeatability: ±0.1nm

*Photometric Readout: Absorbance, %Transmittance, %Reflectance, Energy

*Range: -4.000 to +5.000A; 0 to 999.9%T and %R

*Accuracy: (with NIST 930 Filter) ±0.002A (0 to 0.5A); ±0.004A (0.5 to 1A); ±0.3%T (0 to 100%T)

*Scan Speed: (approx. at 2.0nm)FAST (1233nm/min.), MEDIUM (641nm/min.), SLOW (467nm/min.), SUPER SLOW (310nm/min.)

*Drift: (after 2 hr. warmup) <0.0004A/hr. *Lamps: Halogen (50W), deuterium *Detector: Photomultiplier R-928 *Monochromator: Single *Stray Light: (at 220 and 340nm)<0.015% *Noise: (300nm peak-to-peak)0.0030A

Lidstrom:UV-2401PC UV-Vis recording spectrophotometer

Back to Protocols

About the UV-2401 PC spectrophotometer

Manual

Shimadzu = manufacturer

TUTORIALS:

Basics

The cuvette position in the back is for the reference cell.

Specifications

Wavelength range : 190nm – 1lOOnm (Effective measuring range is 190-900nm)

Spectral band width (slit width): 6 steps in 0.1,0.2,0.5, 1,2, 5

Resolution: O.1 nm

Display of wavelength: 0. 1nm increments

Setting of wavelength: The start wavelength and end wavelength in scanning can be set in increments of 1 nm. With the Goto WL command, wavelength can be set in increments of O.1nm

Wavelength accuracy: + 0.3nm (at slit width of 0.2nm). Automatic wavelength calibration is possible.

Wavelength repeatabihty: plus or minus O.1 nm

Wavelength scanning speed :

Switching of the light sources: The light sources are switched automatically in conjunction with wave-length scanning. The wavelength at which the light sources are switched is selectable in the range of 282nm to 393nm in 0. 1 nm increments.

Stray light:

Photometric system:

Photometric range: Absorbance: – 4 – 5 Abs, Transmittance: 0 – 999.9%T

Recording range: Absorbance: – 9.999 – 9.999 Abs (0.001 Abs of the full scale in maximum expansion), Transmittance: – 999.9 – 999.9%T (0.1% of the full scale in maximum expansion)

Optics

Manual page 3: The light source is turned on by the personal computer under specific conditions, as follows:

When both START and END wavelengths are within the range from 190nm to the switching wavelength, only the D2 lamp will be turned on. When both the START and END wavelengths are within the range from the switching wavelength to 900nm, only the WI lamp will be turned on. When one wavelength falls below the light source switching wavelength and one above, both D2 and WI lamps will be turned on.

In the UV-24OlPC, the positions of the light sources are adjusted automatically, ensuring that maximum intensity is obtained from the detector every time the power switch is turned on.

All the optical elements except light source are sealed from the atmosphere by the windows W, to keep them dust-free. This is one of the features of the UV-2401PC. The slit width is selected

in 6 steps; 0.1, 0.2,0.5, 1, 2,5.

In normal measurement, a slit width of 2nm is considered appropriate.

The monochromator is composed of Sl (entrance slit), M2 (mirror), G (grating), M3 (mirror) and S2 (exit slit). The mounting is of the Czemy-Turner type, characteristically providing little aberration.* The Shimadzu-designed blazed holographic grating with 1600 lines/mm provides high optical energy with minimal stray light.

The images of the exit slit S2 are focused at the cell position in the sample compartment.

Figure 3-5 shows the relationship between the position of cell and light beam. The cross section of the light beam on the cell is about lmm wide and 12mm high when the slit width is 2nm.

When a micro cell of narrow width below 2mm is used, it is recommended that the optional cell holder with mask (P/N 204-06896) or the optional super micro cell holder (P/N 206-14334) can be used. In addition, a black masked cell is preferable for decreasing the influence of the scattered radiation.

Reference Cell

The photometer works to compute the ratio of sample signal to reference signal to obtain the transmittance (T%), to perform baseline correction, logarithmic conversion (into Abs.) and smoothing.

Checking wavelength accuraccy (semi-annually)

Wavelength accuracy is checked using the two characteristic wavelength peaks of deuterium E light, at 486.0nm and 656. If the wavelengths of the characteristic peaks do not fall within the specified ranges, contact your service representative. The procedure is as follows:

Select “Spectrum” from the Acquire Mode menu. Select “Parameters” from the Configure menu. Set the parameters as follows: Measuring Mode : Energy Recording Range : 0 (Low)-100 (High) Wavelength Range : 660 (Start)-650 (End) Scan Speed : Medium Slit Width : 0.2 Sampling Interval : Auto Select the “Energy” push button at the bottom of the Spectrum Parameters dialog box to bring up the Energy Condition Parameters dialog box. Set the parameters as follows: Lamp : D2 (Deuterium) Detector : PM (photomultiplier) PM Gain : 2 Select the “OK” push button to return to the Spectrum Parameters dialog box, and select the “OK” push button to return to the main scree When the photometer setup waiting period ends, select the Start push button to plot the spectrum on the screen graph. When the spectrum has been plotted, a file name and comment may be entered in the File Name dialog box which will appear. Select “Peak Pick” from the Manipulate menu. When the channel selection dialog box appears, select the channel corresponding to the wavelength check spectrum and select “OK”. The graph will be redrawn with the characteristic peak indicated, and the Peak Pick

scrollable window which appears will indicate the wavelength of the peak. The peak wave-length should fall in the range between 655.&m and 656.4nm for UV-2401/25OlPC.

Perform the same procedure again for the other characteristic peak of D2 light using: Recording Range : 0 (Low) – 10 (High) Wavelength Range : 490 (Start) – 480 (End) In this case, the peak wavelength should fall in the range between 485.7nm and 486.3nm for UV-2401/25OlPC.

Kinetic Mode

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